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Synthesis, Growth and Characterization of an Organic Material: P-Chloroanilinium Ethanoate

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Document pages: 16 pages

Abstract: Aromatic organic material of P-Chloroanilinium ethanoate (CAE) has beensynthesized by condensation process using methanol as a solvent. Thesynthesized product is allowed to evaporate slowly at room temperature andcrystals of cell dimension 25 × 29 × 10 mm3 were grown. The grown material wassubjected to single crystal X-ray diffraction to obtain the cell parameters.The presence of functional groups in the grown material was confirmed byFourier transform infrared and Fourier transform Raman spectral studies. TheUV-VIS absorption spectrum reveals that the material has lower UV cut-offwavelength at 337 nm. Using the Kurtz Perry Powder method, the NLO activity wasconfirmed. Mechanical strength of the crystal was estimated by Vickers microhardness test which shows that the material belongs to the soft category. Thethermal behavior of the material was investigated by using thermo gravimetricand differential scanning calorimetric analyses.

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